A successful Jar Test is very reliant upon
the proper preparation of the polymers being tested. Dilution technique
("make down") is especially critical, since it involves compactly
coiled large molecules in emulsions, prior to activation. The polymer must
be uncoiled to provide maximum contact with the colloidal particles to be
flocculated. If the following procedures are not followed, the Jar Test
results will be very unreliable.
- Required equipment:
- 250 mL bottles with lids.
- High speed hand mixer (for emulsion polymers).
- Syringes (1cc, 5cc, 10cc).
- 250 and 500 mL beakers.
- Water (it is recommended that the makedown
water from the plant be used).
- Graduated cylinder (100 mL).
- Emulsion polymers (Prepare 1.0% solution.)
- Add 198 mL of water to a beaker.
- Insert Braun mixer into water and begin
mixing.
- Using a syringe, inject 2 mL of neat polymer
into vortex.
- Mix for 20 seconds. Do not exceed 20 seconds!
- Allow dilute polymer to age for at least
20 minutes, but preferably overnight.
Prepare 0.1% solution.
- Add 180 mL of water to 250 mL bottle.
- Add 20 mL of 1.0% polymer solution.
- Shake vigorously for at least one minute.
- Solution polymers and Inorganics (Prepare a 1.0% solution.)
- Add 198 mL of water to 250 mL bottle.
- Using a syringe, add 2 mL of neat product
to bottle.
- Shake vigorously for at least 1 minute.
- Prepare 0.1% solution.
- Add 180 mL to 250 mL bottle.
- Add 20 mL of 1 % solution.
- Shake vigorously for at least one minute.
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